PDF SUPPORTING INFORMATION Radical reduction of alkyl and aryl halides ...
stainless steel ball bearing. A Teflon gasket was added and the vial sealed and placed in a Spex 8000 mixer mill. The reaction was shaken for 2 hours at 18 hertz and at 120 oC. The crude reaction mixture was recrystallized with approximately 2 mL of acetone to isolate adamantane. 1HNMR, 13C NMR and GCMS